Chemistry at Nanometre Scale (B-KUL-H06A6A)

6 ECTSEnglish56 Second termCannot be taken as part of an examination contract
De Feyter Steven (coordinator) |  De Feyter Steven |  N. |  Mali Kunal (substitute)
POC Nanowetenschappen en nanotechnologie

The student must be able

  • to explain the concepts of nanochemistry by hard
  • to compare the different approaches to make and analyse nanomaterials
  • to use concepts of nanochemistry to address research questions
  • to apply the concepts for the formation and characterization of new nanomaterials
  • to analyse and understand concepts discussed in recent scientific literature
  • to carry out basic experiments under guidance
  • to link experiment with theory

Necessary basis to disciplines as offered in the introductory courses H06F6A Structure synthesis and cellular function of macromolecules; H09M2A Atomtheory, chemical periodicity and chemical bond. Basic knowledge of bio-organic chemistry, physical chemistry, and material science.


This course unit is a prerequisite for taking the following course units:
H06N2A : Lectures on Nanoscience and Nanotechnology
H06L6B : Project Work Nanoscience (No longer offered this academic year)
H0P61A : P&O Nanoscience, Nanotechnology and Nanoengineering
H0P62A : Projectwerk nanowetenschappen, nanotechnologie en nanoengineering

This course is identical to the following courses:
H05K8A : Chemie op nanometerschaal

Activities

4.8 ects. Chemistry at Nanometre Scale: Lecture (B-KUL-H06A6a)

4.8 ECTSEnglishFormat: Lecture36 Second term
POC Nanowetenschappen en nanotechnologie

A. Introduction

        Chapter 0: Introduction
        Chapter 1: Nanosafety

B. Supramolecular Chemistry and Self-Assembly: from Covalent to Non-Covalent Chemistry

        Chapter 2: Supramolecular Chemistry – Molecular Recognition
        Chapter 3: Self-Assembly
        Chapter 4: Self-Assembly in Water
        Chapter 5: Self-Assembly: Stabilization
        Chapter 6: Large Building Blocks
        Chapter 7: Liquid Crystals
        Chapter 8: Biomineralisation
        Chapter 9: Nanomotors

C.  Organisation of Matter on Surfaces at the Nanometer Scale

        Chapter 10: Scanning Probe Microscopy
        Chapter 11: Langmuir-Blodgett Films
        Chapter 12: Layer-by-Layer Deposition
        Chapter 13: Self-Assembled Monolayers
        Chapter 14: Soft-Lithography
        Chapter 15: Molecular Nanopatterns
        Chapter 16: Block Copolymers

D.    Chapter 17: Microporous and Mesoporous Materials

E. Nanoparticles (preparation / properties)

        Chapter 18: Nanocrystals
        Chapter 19: Nanotubes – Nanorods – Nanowires

F. 2D nanomaterials

        Chapter 20: 2D Materials
       

Course material is available on Toledo. 

There is also the option to order black-and-white copies.

Recommended reading (review papers) will be provided as pdf-files.

Part of the course material is based upon the books"Nanochemistry: A Chemical Approach to Nanomaterials" (ISBN 978-1-84755-895-4) and "Concepts of Nanochemistry" (ISBN 978-3-527-32626-6). This is recommended reading, but is not required.

content is mainly lectured ex cathedra

1.2 ects. Chemistry at Nanometre Scale: Exercises and Laboratory Sessions (B-KUL-H06A7a)

1.2 ECTSEnglishFormat: Practical20 Second term
De Feyter Steven |  N. |  Mali Kunal (substitute)
POC Nanowetenschappen en nanotechnologie

Exercise sessions: to get familiar with the concepts of nanochemistry, and to apply them.

Lab sessions: to get hands-on experience with the synthesis and characterisation of nanomaterials

Tasks:  related to the study/discussion of recent scientific literature on a Nanochemistry related subject dealing with your specific field of study

Instructions on exercise sessions, lab sessions, and tasks on Toledo.

Exercise sessions:
There are typically two exercise sessions 
The exercise questions are typically exam questions from previous years.
The exercise sessions give the opportunity to the student to evaluate her or his depth of understanding
Timing of the exercise sessions is communicated during the semester

Lab session:
The lab session will be organized towards the end of the semester. The duration is between 2 and 3 hours.
Participation is mandatory.
5% of the marks of this course are based on the lab session.
The lab session is evaluated by handing in a set of answers on questions at the start and at the end of the lab session. Students are required to prepare. They receive the description of the lab exercises well in advance. 

Tasks:
Literature study (2 parts) on scientific literature on a nanochemistry related subject dealing with the student’s specific field of study or interest.
Part 1: The student must select from the recent scientific literature (current academic year), a peer reviewed paper in a specific domain of interest, related to "nanochemistry". The student must summarize in English the important points of this paper, and express his or her specific interest in the selected paper. The student must discuss the potential 'nanotoxicity' issues, if relevant and list a number of (scientific) questions or statements related to the paper.
Part 2: The student evaluates the paper and report of a fellow student, and looks for links with her or his specific field of study or interest
15% of the marks of this course are based on the tasks
Timing is communicated at the start of the course. The deadlines for submission of the tasks are approximately  9 (part 1) and 13 weeks (part 2) after the start of the course.

Evaluation

Evaluation: Chemistry at Nanometre Scale (B-KUL-H26A6a)

Type : Partial or continuous assessment with (final) exam during the examination period
Description of evaluation : Oral, Report
Type of questions : Multiple choice, Open questions
Learning material : Course material


The evaluation is based on an exam, and tasks and a lab session (participation obligatory) during the semester. If for reasons of force majeure, the on-campus laboratory session(s) cannot go ahead in their current form, compulsory attendance will be waived. The laboratory session(s) will be replaced by an additional task. 

Task(s): 15% 

Lab session: 5% (particiption in the lab session as schedudled is a requirement to take the exam, also for retaking the exam (except if your absence is legal))

Exam: 80%

The exam is an 'open book' exam. 

- There is no chance to (re)do the lab session or to (re)do the tasks in the same academic year. The marks obtained for the tasks and lab session are transferred (total 20%)